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Development of a Spectrophotometric Method for the Quantitative Estimation of Zidovudine Concentration in Bulk and Pharmaceutical Dosage Forms

Development of a Spectrophotometric Method for the Quantitative Estimation of Zidovudine Concentration in Bulk and Pharmaceutical Dosage Forms

Original Research ArticleMar 30, 2018Vol. 10 No. 1 (2010)

Abstract

A simple, accurate, precise, sensitive and a highly selective spectrophotometric method was developed and validated for the estimation of Zidovudine in bulk and pharmaceutical dosage forms. The stock solutions were prepared as per procedure and were scanned at maximum absorbance of 266 nm. The linearity was found in the concentration range of 2-20 µg / mL. The Coefficient of determination (r2) was 0.999. The regression equation was found to be Y = 0.0435. C + 0.0205 and % RSD was found to be 0.630. The developed method was validated according to ICH guidelines and was found to be accurate and precise. The validation parameters are linearity, accuracy, precision, limit of detection, limit of quantitation, robustness and ruggedness. Thus the proposed method can be successfully applied for the estimation of Zidovudine in bulk and pharmaceutical dosage forms.

 

Keywords: Zidovudine, Validation, ICH guidelines, Spectrophotometric method

*Corresponding author: Mobile Phone: 08978304042

E-mail: chejetisharadha@gmail.com

How to Cite

Sharada*, C. H. ., Channabasavaraj, K. P. ., & Mani, T. T. . (2018). Development of a Spectrophotometric Method for the Quantitative Estimation of Zidovudine Concentration in Bulk and Pharmaceutical Dosage Forms. CURRENT APPLIED SCIENCE AND TECHNOLOGY, 1-8.

References

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  • [4] United States Pharmacopoeia (USP-NF XXIV), 1985. Rockville MD 20852. United States Pharmacopoeial Convention Inc, p. 3489.
  • [5] Bengi Uslu and Sibel A Ozkan, 2002. Determination of Lamivudine and Zidovudine in binary mixtures using First Derivative Spectrophotometric, first derivative of the ratio-spectra and HPLC-UV methods, Analytical Chemica Acta, 466 (1), 175-185.

Author Information

C. H. Sharada*

Department of Pharmaceutical Analysis, Bharathi College of Pharmacy, Bharathi Nagara, Karnataka, India

K. P. Channabasavaraj

Department of Pharmaceutical Analysis, Bharathi College of Pharmacy, Bharathi Nagara, Karnataka, India

T. Tamizh Mani

Department of Pharmaceutical Analysis, Bharathi College of Pharmacy, Bharathi Nagara, Karnataka, India

About this Article

Journal

Vol. 10 No. 1 (2010)

Type of Manuscript

Original Research Article

Keywords

Zidovudine, Validation, ICH guidelines, Spectrophotometric method

Published

30 March 2018